Tetrahydrofuran

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Tetrahydrofuran (unstab.) ULC/MS - Suitable GPC analysis 1

Test Specification Result
Clear colorless liquid Complying Complying
Color ( APHA Pt – Co ) < = 10 5
Assay ( T dry ) 99.95 – 100.10 % w / w 100.00 % w / w
Water ( KF ) < = 0.02 % w / w 0.01 % w / w
UHPLC / MS ESI / APCI + ( 0.1 % as Reserpine ) < = 20 ppb < 10 ppb
Grad . elution H.Peak at 254nm < = 0.002 AU < 0.001 AU
Grad . elution drift at 254nm < = 0.010 AU 0.004 AU
UV Trans . 260nm > = 10 % 17%
UV Trans . 270nm > = 79 % 87%
UV Trans . 280nm > = 93 % 97%
UV Trans . 300nm > = 95 % 98%
UV Trans . 320nm > = 96 % 98%
Fluorescence 254nm ( 25 % as Quinine ) < = 1 ppb < 1 ppb
Fluorescence 365nm ( 25 % as Quinine ) < = 1 ppb < 1 ppb
Aluminum ( Al ) < = 0.05 ppm < 0.05 ppm
Calcium ( Ca ) < = 0.2 ppm < 0.2 ppm
Iron ( Fe ) < = 0.3 ppm 0.3 ppm
Potassium ( K ) < = 0.1 ppm 0.1 ppm
Magnesium ( Mg ) < = 0.05 ppm 0.05 ppm
Sodium ( Na ) < = 0.5 ppm 0.5 ppm
Residue after evaporation < = 0.001 % w / w < 0.001 % w / w